How do you calculate the percentage of sodium bisulphite using titration?

In summary, sodium bisulphite titration is a chemical analysis technique used to determine the concentration of an oxidizing agent in a solution. It involves the addition of sodium bisulphite, a reducing agent, to the solution until the reaction is complete. The purpose of this titration is to obtain precise control of the concentration of the oxidizing agent, which is important in industries such as water treatment, food and beverage production, and pharmaceuticals. To perform this titration, a burette, standard solution of sodium bisulphite, indicator solution, beaker or flask, and volumetric flask are needed. The process involves adding increments of the standard solution and indicator to the solution being titrated until the endpoint is reached,
  • #1
barryfol
1
0
Hi all,

i am hoping to make sodium bisulphite by passing so2 through NaOH.

However, i was wondering if anyone has a link or a method to a titration for calaulating % sodium bisulphite,

Regards,
 
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  • #2
It is usually titrated with iodine. Try googling "iodine titration of sulfite bisulfite". Many many hits. You may need to consult an analytical chemistry textbook for details.
 
  • #3


Hello,

To calculate the percentage of sodium bisulphite in your solution, you will need to perform a titration using a standardized solution of iodine. Here is a general method for conducting a sodium bisulphite titration:

1. Prepare your sodium bisulphite solution by passing SO2 gas through NaOH until it is fully saturated.

2. Using a volumetric flask, dilute a known volume of your sodium bisulphite solution with distilled water.

3. Add a few drops of starch indicator to your diluted solution.

4. Using a burette, slowly add your standardized iodine solution to the diluted sodium bisulphite solution until the solution turns blue. This indicates that all of the sodium bisulphite has reacted with the iodine.

5. Record the volume of iodine solution used.

6. Repeat the titration two more times and calculate the average volume of iodine solution used.

7. Use the following equation to calculate the percentage of sodium bisulphite in your solution: % Sodium Bisulphite = (Volume of Iodine Solution x Molarity of Iodine Solution x 100) / Volume of Sodium Bisulphite Solution

I hope this helps! Good luck with your experiment.
 

What is sodium bisulphite titration?

Sodium bisulphite titration is a chemical analysis technique used to determine the concentration of a substance (usually an oxidizing agent) in a solution. It involves the addition of sodium bisulphite, a reducing agent, to the solution until the reaction is complete. The amount of sodium bisulphite used is then used to calculate the concentration of the oxidizing agent.

What is the purpose of sodium bisulphite titration?

The purpose of sodium bisulphite titration is to determine the concentration of an oxidizing agent in a solution. This information can be useful in various industries, such as water treatment, food and beverage production, and pharmaceuticals, as it allows for precise control of the concentration of the oxidizing agent.

What materials are needed for sodium bisulphite titration?

The materials needed for sodium bisulphite titration include a burette, a standard solution of sodium bisulphite, an indicator solution (such as starch or iodine), a beaker or flask to hold the solution being titrated, and a volumetric flask to prepare and store the solution being titrated.

What is the process of sodium bisulphite titration?

The process of sodium bisulphite titration involves adding small increments of the standard sodium bisulphite solution to the solution being titrated, while also adding the indicator solution. The endpoint of the titration is reached when the indicator changes color, indicating that the reaction is complete. The amount of sodium bisulphite used can then be used to calculate the concentration of the oxidizing agent.

What are the sources of error in sodium bisulphite titration?

Some potential sources of error in sodium bisulphite titration include inaccurate measurement of the solutions, improper mixing or agitation, and variations in the endpoint determination due to differences in color perception. It is important to carefully follow the procedure and use precise measuring equipment to minimize these sources of error.

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