What factors can affect the efficiency of soxhlet extraction?

In summary, the conversation discusses a problem with the soxhlet extraction cycle. The liquid in the middle section of the apparatus should return to the bottom section, but it did not happen in the whole cycle even though the liquid level reached the appropriate height. There is a questioning of whether the solvent volume changed and if the soxhlet extraction procedure is temperature dependent. The speaker also suggests that variables such as temperature and viscosity may affect the experimental outcomes.
  • #1
Patty
1
0
I have a trouble with soxhlet extraction cycle.
Liquid in the middle section of soxhlet appratus should returen to the bottom section of soxhlet appratus when it reaches an appropriate height. The question is :The return did not appearence in the whole cycle but the liquid level actually reached that height.
 
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  • #2
Did the solvent volume change?
 
  • #3
soxhelt extraction procedure?Why?

march.12.2004
Is your procedure temperature dependent for extraction,if so volume at that temperature would had been altered.Also the viscosity must be altered.I do not actually know your specific experiment but being a physical chemis i guess possible variables which might affect experimental outcopmes.
 

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