Recent content by acvtre
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HVAC DIY glovebox or closed fume-hood?
Hi everybody, I'm a PhD student working on solution-processed kesterite PV cells. The material is spin-coated and I personally believe that its wetting properties are influenced by environmental parameters like temperature and humidity. To control these parameters, or at least reduce their...- acvtre
- Thread
- Closed Control Diy Humidity
- Replies: 2
- Forum: DIY Projects
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UV-Vis Amine Problem: Solutions & Explanations
I'm trying different solutions and one of these has 0.1% of ethanolamine as a suspension agent, right.- acvtre
- Post #13
- Forum: Materials and Chemical Engineering
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UV-Vis Amine Problem: Solutions & Explanations
Aaaaaand here it is: I've done the analyses as you suggested with a solution of water + ethanolamine with a 20% and 40% concentration and acetonitrile as background. As you can see there's a big absorbance at 225nm. So I think this one is the cut-off wavelength of the ethanolamine. In my...- acvtre
- Post #11
- Forum: Materials and Chemical Engineering
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UV-Vis Amine Problem: Solutions & Explanations
- I use the UV-vis spectrophotometer in order to find out if I got GIZO nanoparticles in different solutions, to do so, I always use a reference background, wavelength scan from 600nm to 200nm and what I need to see is a peak between 205-210nm. - I really don't know what is the lambda max of...- acvtre
- Post #9
- Forum: Materials and Chemical Engineering
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UV-Vis Amine Problem: Solutions & Explanations
All the solutions give me a peak around 210nm, which is the nanoparticle peak, I alwasy use the background. Only the ethanolamine gives me a weird result, even though I use the background, which is a non-sense. As I've written, also when I use only ethanolamine I get the same weird results...- acvtre
- Post #7
- Forum: Materials and Chemical Engineering
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UV-Vis Amine Problem: Solutions & Explanations
I encountered this problem with a solution that only had 0.1% of ethanolammine. In particular, my analyte was composed by: GIZO nanoparticles dispersed in ethylene glycol, pentanol, PVA and ethanolammine. As I had the negative absorbance I analyzed the ethanolamine as analyte on itself, with...- acvtre
- Post #5
- Forum: Materials and Chemical Engineering
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UV-Vis Amine Problem: Solutions & Explanations
Yes, it is a double beam, infact I've got one space for the for the reference and another one for the sample to analyze. For what I understand the baseline is constant and what I see is a peak that goes below it. I've got this problem only with the amines. I've tried with pure ethanolamine and...- acvtre
- Post #3
- Forum: Materials and Chemical Engineering
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UV-Vis Amine Problem: Solutions & Explanations
Good day to everybody, I immediately expose my problem. I'm doing some measurements with the UV-vis spectroscopy and I'm having problems with the amines in the non visible region. This is what I do: put my amine in a quartz cuvette -> do the background (reference) -> analyze the same solution...- acvtre
- Thread
- Analysis Spectrocopy Uv light
- Replies: 12
- Forum: Materials and Chemical Engineering