Schwartz reagent-- NMR/MS/IR

cep

Hi Everyone,

I'm looking for some spectral data on Schwartz reagent (ZrCp2ClH); at the very least, I'd like to find a 1H NMR spectrum, but I would also like to see mass spec and IR spectra. I have had zero luck finding a paper that reports characterization data of the reagent itself. I've used ISI, SciFinder and Reaxys. Anyone know of any papers or textbooks?

Thanks,

-Carol

sjb-2812

Something like http://www.orgsyn.org/orgsyn/orgsyn/...?prep=cv9p0162 ?