Where Can I Find Spectral Data for Schwartz Reagent (NMR/MS/IR)?

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SUMMARY

The discussion centers on the search for spectral data of Schwartz reagent (ZrCp2ClH), specifically 1H NMR, mass spectrometry (MS), and infrared (IR) spectra. The user, Carol, has utilized databases such as ISI, SciFinder, and Reaxys without success in locating relevant characterization data. A suggestion was made to refer to a specific organic synthesis resource, indicating that such data may be available through specialized publications or databases.

PREREQUISITES
  • Understanding of NMR spectroscopy principles
  • Familiarity with mass spectrometry techniques
  • Knowledge of infrared spectroscopy fundamentals
  • Experience with scientific databases like SciFinder and Reaxys
NEXT STEPS
  • Search for spectral data in specialized organic chemistry journals
  • Investigate the organic synthesis resource mentioned: http://www.orgsyn.org/orgsyn/orgsyn/prepContent.asp?prep=cv9p0162
  • Explore the use of chemical databases for spectral data retrieval
  • Review literature on ZrCp2ClH for any related studies or characterization reports
USEFUL FOR

Chemists, researchers in organic synthesis, and anyone involved in the characterization of chemical compounds, particularly those working with transition metal reagents.

cep
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Schwartz reagent-- NMR/MS/IR

Hi Everyone,

I'm looking for some spectral data on Schwartz reagent (ZrCp2ClH); at the very least, I'd like to find a 1H NMR spectrum, but I would also like to see mass spec and IR spectra. I have had zero luck finding a paper that reports characterization data of the reagent itself. I've used ISI, SciFinder and Reaxys. Anyone know of any papers or textbooks?

Thanks,

-Carol
 
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