Titanium dioxide solution in oil

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The discussion centers on creating a stable titanium dioxide (TiO2) suspension in oil, specifically using Tronox CR828, Isopar M, and sorbitan trioleate. The main issue is that the mixture clumps and settles after homogenization, indicating instability. Participants note that this is a colloidal suspension rather than a true solution, and stability depends on factors like particle size. There is a suggestion to explore the use of a suitable dispersant or anti-settling agent to improve stability. Additionally, the potential for formulating a microencapsulated suspension with TiO2 and Fe3O4 nanoparticles is mentioned, with a request for expert assistance in identifying effective dispersants. The conversation also touches on the viscosity of the solvent, suggesting that a thicker fluid might enhance stability.
SaketIndra
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Hello everyone,

I am seeking assistance in preparing a Titanium dioxide solution in oil. Below are the chemical compositions of the solution:

  1. Titanium Dioxide (TiO2): 20% by weight, with the product name Tronox CR828.
  2. Solvent/Oil: Isoparaffin, constituting 75% by weight, with the product name ISOPAR M.
  3. Surfactant: Sorbitan trioleate, comprising 5% by weight.
However, I am encountering an issue where the solution clumps together and settles down in the beaker after homogenization. I'm unsure of what I might be doing wrong.
 
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Technically it is not a solution, but a suspension (or a colloid). Whether it is stable or not depends (between other factors) on the suspended particles size.

Are you 100% sure the recipe guarantees a stable mixture and calls for exactly these brands of components? Such things tend to be highly erratic.
 
Borek said:
Technically it is not a solution, but a suspension (or a colloid). Whether it is stable or not depends (between other factors) on the suspended particles size.

Are you 100% sure the recipe guarantees a stable mixture and calls for exactly these brands of components? Such things tend to be highly erratic.
Hello, you're absolutely correct. This refers to a colloidal solution where TiO2 is intended to be suspended. After conducting some research, I have focused on formulating a microencapsulated suspension of TiO2 and Fe3O4 nanoparticles for use in magnetophoretic displays.
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While I understand the necessity of using a suitable dispersant and anti-settling agent, I'm facing difficulties in identifying the most appropriate options. If you happen to know any interested individuals or experts, I would be grateful if you could provide their information. I am willing to create a freelancing job request on their preferred platform, and they can assist me in this matter. Please inform me if you have any leads.
 
Isopar M is a fairly low viscosity fluid. Have you tried using something thicker?

Have you tried adding the Fe3O4 to the mixture that you have created and encapsulating it? It may have different properties in that physical configuration.

BoB
 
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