What is the right amount of citric acid and sodiumhypophosphite?

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SUMMARY

The discussion centers on the correct measurements of citric acid and sodium hypophosphite for a starch solution. The article specifies using 5% citric acid based on the starch weight, which translates to 1.28 grams for 3 grams of starch. Additionally, sodium hypophosphite should be weighed at 50% of the citric acid amount, resulting in 0.64 grams. The confusion arises from the differing percentages mentioned in the article, but the calculations provided align with the specified concentrations.

PREREQUISITES
  • Understanding of weight/weight (w/w) percentage calculations
  • Knowledge of starch solution preparation
  • Familiarity with citric acid and sodium hypophosphite as chemical reagents
  • Basic laboratory weighing techniques
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  • Research the role of citric acid in cross-linking starch solutions
  • Learn about the properties and applications of sodium hypophosphite as a catalyst
  • Explore methods for preparing and measuring chemical solutions accurately
  • Investigate the effects of varying citric acid concentrations on starch film properties
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Chemistry students, researchers in materials science, and professionals involved in polymer chemistry or food science will benefit from this discussion.

Cyrus the great
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Homework Statement



In the materrials and methods of one article is mentioned that: A specific amount of citric acid and the catalyst sodium hypophosphite (50 % w/w, on weight of citric acid used) was dissolved in the starch solution.

My question is how much citric acid and sodium hypophosphite I need to weigh on the balance?

p.s: In one part of article is written: Films were cast from 3 % starch and cross-linked using 5 % (w/w) citric acid.

Homework Equations

The Attempt at a Solution



50 % w/w so we need to weigh 50 g or mg of citric acid + 50 g or mg of sodium hypophosphite.

But why in another part of article mentioned 5 % of citric acid was used? I am confused![/B]
 
Last edited:
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I calculated like this. I want to make 3 % of starch so I weigh 3 gram of starch. Then 5 % of citric acid which is 1.28 gram then catalyst 50 % which becomes 0.64 gram. Then I will add 96.23 gram of water. Am I right?
 
Any feedback?
 

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