Calculating Weight Loss Rate: TGA/DSC Measurements

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Discussion Overview

The discussion revolves around calculating the rate of weight loss using TGA (Thermogravimetric Analysis) and DSC (Differential Scanning Calorimetry) measurements. Participants are exploring how to define the initial mass for calculations and the implications of using different mass values over time.

Discussion Character

  • Exploratory
  • Technical explanation
  • Debate/contested

Main Points Raised

  • One participant questions whether to use the initial mass consistently (m0) or to adjust it based on previous mass measurements (e.g., m3-m2, m4-m3) for calculating weight loss rate.
  • Another participant suggests that the choice depends on whether the graph should represent the weight lost each second or the total weight lost since the beginning of the measurement.
  • A third participant states that the instantaneous rate of mass loss (dm/dt) is typically the useful quantity, implying that the slope of the mass curve should be used for calculations.
  • A separate post offers TGA and DSC measurement services, indicating a commercial aspect to the discussion.

Areas of Agreement / Disagreement

Participants express differing views on the appropriate method for calculating weight loss rate, indicating that there is no consensus on whether to use the initial mass or adjust based on previous measurements.

Contextual Notes

Participants have not fully resolved the implications of their choices on the shape of the plotted graph or the specific context in which each calculation method is most appropriate.

Who May Find This Useful

Researchers and practitioners involved in TGA and DSC measurements, as well as those interested in the analysis of weight loss rates in materials science.

Oxygenne
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I want to calculate the rate of weight loss and not sure should I keep the initial mass at the initial time always or should I use the previous mass of recorded data

should be m0 as inital value always or is should change to m3-m2, m4-m3, in this way.

I plotted the graph and it does not have a similar shape so i have to make a choice but I am confuse.

I look forward to your advise. Thank you!
 
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Oxygenne said:
I want to calculate the rate of weight loss and not sure should I keep the initial mass at the initial time always or should I use the previous mass of recorded data

should be m0 as inital value always or is should change to m3-m2, m4-m3, in this way.

I plotted the graph and it does not have a similar shape so i have to make a choice but I am confuse.

I look forward to your advise. Thank you!
It depends on what you want. Do you want to see, on your graph, the weight that is lost each second, or the weight that have been lost since the beginning of the run?

TP
 
It is usually the instantaneous rate of mass loss (dm/dt) that is the useful quantity, and therefore the slope of the mass curve is what one typically uses.
 

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