How Did Chemists of the Past Measure Elements for the Periodic Table

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Discussion Overview

The discussion revolves around how chemists in the past measured the weights of elements to construct the periodic table without modern laboratory techniques. It explores methods used for determining atomic weights, the identification of elements versus compounds, and the historical context of these practices.

Discussion Character

  • Exploratory
  • Technical explanation
  • Historical

Main Points Raised

  • One participant inquires about the methods used by past chemists to determine atomic weights without modern techniques, suggesting the use of Avogadro's law.
  • Another participant mentions the use of quality balances and acknowledges the role of guesswork in early measurements.
  • There is a question about how chemists ensured they were comparing the same number of particles when measuring atomic weights.
  • A participant asserts that equivalent masses are relative and do not require knowing the exact number of particles in a mole.
  • Another participant challenges this by stating that without knowing the number of atoms, one cannot accurately calculate relative atomic weights from different elements.
  • One participant explains that the ratio of equivalent weights can be determined by examining how much one element reacts with another, linking this to molar masses and valency.
  • A historical note is made about Dalton's contributions to atomic weights, highlighting that some of his values were correct while others were not.
  • Participants discuss alternative methods for inferring the amount of moles, such as freezing point depression and boiling point elevation in solutions.

Areas of Agreement / Disagreement

Participants express differing views on the necessity of knowing the number of particles in a mole for calculating atomic weights. While some argue that equivalent masses are sufficient, others maintain that accurate comparisons require knowledge of atomic quantities. The discussion remains unresolved regarding the best methods used historically.

Contextual Notes

There are limitations in the assumptions made about the methods of measurement and the definitions of elements versus compounds, as well as the historical accuracy of atomic weights proposed by early chemists.

scientifico
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Hello, how did chemists of the past know the weight of the elements to build up the periodic table without using new lab tecniques ?
Have they transformed all the elements into gases and used Avogadro's law to obtain a relative atomic mass ? And how did they it was an element and not a compost ?

Thank you
 
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They used quality balances to measure weight, and a lot of guesswork.

Some composite substances were considered elements till they were proved to be not.
 
Borek said:
They used quality balances to measure weight, and a lot of guesswork.
Yes but to compare atomic weight of two elements you must be sure you have the same number of particles in both elements, how did they solved this ?
 
What exactly do you mean with "whithout using new lab techniques"?
 
withou the possibility to calculate the number of particles in a mole
 
You don't need that, equivalent masses are relative.
 
Borek said:
You don't need that, equivalent masses are relative.
What do you mean?
If I take 1 g of Fe and 1g of S I can't calculate relative atomic weight because they don't contains the same quantity of atoms...
 
Dalton was the first to propose and publish a system of atomic weights.

Google "Dalton atomic weights" finds lots.

However he was right about some and wrong about other weights, as were those who followed immediately.

The story of how the correct values gradually unfolded is quite fascinating and well presented in the book

"Chasing the Molecule" by Julian Buckingham
 
  • #10
You don't need to have vapours. You can also infer the amount of moles e.g. from freezing point depression of solutions of salts, boiling point increase etc.
As others pointed out before, a lot can be learned from studying the mass proportions in different compounds.
 
  • #11
DrDu said:
You can also infer the amount of moles e.g. from freezing point depression of solutions of salts, boiling point increase etc.
What are that ?
 
  • #12
scientifico said:
What are that ?

Have you tried to google them or do you expect to be spoon feed all the time?
 

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