How to convert Antimony Sulfate to Sb2O3?

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Discussion Overview

The discussion revolves around the conversion of Antimony Sulfate to Antimony Trioxide (Sb2O3) for use as a refining and reducing agent in glass melting processes. Participants explore various methods and considerations related to this conversion, including thermal decomposition and hydrolysis.

Discussion Character

  • Exploratory
  • Technical explanation
  • Debate/contested
  • Experimental/applied

Main Points Raised

  • One participant expresses uncertainty about whether Antimony Sulfate will decompose into Sb2O3 at high temperatures (around 1200 Celsius).
  • Another participant suggests that heating Antimony Sulfate will likely lead to its decomposition into Antimony (III) Oxide and Sulfur Trioxide.
  • A different viewpoint proposes that Antimony Sulfate could hydrolyze in dilute water to form the oxide, although this process is described as potentially messy.
  • Some participants discuss the possibility of using calcium or barium hydroxide to precipitate Sb oxide or hydroxide from the sulfate solution.
  • One participant notes that Antimony oxide serves as a reducing agent for manganese and chromium oxides in glassmaking, emphasizing its importance for achieving specific colors in glass.
  • Another participant shares their apprehension about handling Antimony in aqueous form and considers adding a small percentage of Antimony Sulfate to their glass batch instead.
  • One participant expresses frustration at being unable to find Antimony Trioxide for purchase, indicating a reliance on the sulfate instead.

Areas of Agreement / Disagreement

Participants present multiple competing views on the conversion process, with no consensus reached regarding the best method or the effectiveness of the proposed approaches.

Contextual Notes

Some limitations include the uncertainty about the thermal stability of Antimony Sulfate, the conditions under which hydrolysis occurs, and the potential risks associated with handling Antimony in aqueous solutions.

Panthera Leo
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How to convert Antimony Sulfate to Sb2O3?

Hi,

I have got some Antimony Sulfate and would like to convert it to Sb2O3 to be used as a refining & reducing agent in glass melt. But I am not sure if using the sulfate as such will decompose in the oxide at high temperatures (around 1200 celsius)... Any help will be highly appreciated.

Is there any other reducing agent you could recommend?

Thanks.
 
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Heating Antimony Sulphate will likely decompose it to Antimony (III) Oxide and Sulphur Trioxide.
 


It is supposed to hydrolyze in dilute water to the oxide. Sounds messy to me. Why don't you just get some antimony trioxide instead?
 


Panthera Leo said:
I have got some Antimony Sulfate and would like to convert it to Sb2O3 to be used as a refining & reducing agent in glass melt. But I am not sure if using the sulfate as such will decompose in the oxide at high temperatures (around 1200 celsius)... Any help will be highly appreciated.
Is there any other reducing agent you could recommend?
Why reducing? In the sulfate, Sb is in which oxidation state?
Anyway, if the sulfate is water soluble and gives Sb ions and SO42- ions, you could add Ca(OH)2 or, better, Ba(OH)2 (more soluble) and calcium or barium sulfate precipitates giving Sb oxide or hydroxide (or antimonic acid?) and in case you dry the last by heat.
 


Antimony oxide acts as a reducing agent towards manganese and chromium oxides in glassmaking.
 


lightarrow said:
if the sulfate is water soluble and gives Sb ions and SO42- ions, you could add Ca(OH)2 or, better, Ba(OH)2 (more soluble) and calcium or barium sulfate precipitates giving Sb oxide or hydroxide (or antimonic acid?) and in case you dry the last by heat.

Thanks for the instructions... sounds very interesting indeed...

But I am really scared of touching Sb in aqueous state. I guess I will just add a 0.5% of glass batch the Sb sulfate and see what happens :D
 


chemisttree said:
Antimony oxide acts as a reducing agent towards manganese and chromium oxides in glassmaking.

You're 100% correct :)

without Sb2O3 it's almost impossible to create deep/pure green colors (from Cr2O3) generally because sodium oxide and chromium oxide react to form sodium chromate which gives the glass a yellowish tint.

If there's a tiny amount of PbO in the batch, lead chromate will form making the glass brownish orange instead of green !

Both cases can be avoided with the addition of Sb2O3...
 


chemisttree said:
It is supposed to hydrolyze in dilute water to the oxide. Sounds messy to me. Why don't you just get some antimony trioxide instead?

I wish, I could ... I have searched every single chemical shop in town but non of them is offering the oxide for sale! all I could find was the sulfate.
 

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