- #1
Oxygenne
- 51
- 0
I am doing XRF analyses and in situ HTXRD, there is Topas available.
Actually the experiment it is not done by me because I was told only one person should run the instrument in order to not damage it.
I asked
- to have 2 theta but the person told to me “no. all the people get results in this form.”
- to get the raw file and the ASCI file
- to get the pdf file in text format in order to know what is the descriprion in the matched file
- I file a sample of report after the experiment asking to include
“? wavelength dispersive X-ray fluorescence spectrometer, operated using a ? kW tube at ? kV and ? mA”
“? XRD diffractometer using ?radiation in ? mode with ? degree step size and ? s/step sampling time. The powder sample was placed ?. The samples were heated to various temperatures a heating rate of ? C/min and were held at various temperatures for ? min before recording the spectra.
match with the JCPDS file no ?”
Also since Topas is available I asked to get the the crystallite size calculations
But at the end I get the results with the d on the x-axis emf format paint-file and in one corner is listed the name of matched compounds.
To all above mentioned I was told you do not need that or we do not do that.
Would you please let me know why I do not get the results in detail as I asked?
Is it something wrong in my request from the scientific point of view?
Thank you.
Actually the experiment it is not done by me because I was told only one person should run the instrument in order to not damage it.
I asked
- to have 2 theta but the person told to me “no. all the people get results in this form.”
- to get the raw file and the ASCI file
- to get the pdf file in text format in order to know what is the descriprion in the matched file
- I file a sample of report after the experiment asking to include
“? wavelength dispersive X-ray fluorescence spectrometer, operated using a ? kW tube at ? kV and ? mA”
“? XRD diffractometer using ?radiation in ? mode with ? degree step size and ? s/step sampling time. The powder sample was placed ?. The samples were heated to various temperatures a heating rate of ? C/min and were held at various temperatures for ? min before recording the spectra.
match with the JCPDS file no ?”
Also since Topas is available I asked to get the the crystallite size calculations
But at the end I get the results with the d on the x-axis emf format paint-file and in one corner is listed the name of matched compounds.
To all above mentioned I was told you do not need that or we do not do that.
Would you please let me know why I do not get the results in detail as I asked?
Is it something wrong in my request from the scientific point of view?
Thank you.