Instrumental line broadening of Rigaku smartlab

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SUMMARY

The discussion centers on determining the instrumental line broadening of the Rigaku SmartLab diffractometer. Users suggest measuring reference samples such as LaB6, Si, and Al2O3 to fit the resolution function, which is essential for obtaining accurate line broadening data. Additionally, well-characterized standard materials can be sourced from NIST to aid in this process. Understanding the resolution function is crucial for interpreting the XRD patterns obtained from these samples.

PREREQUISITES
  • Familiarity with X-ray diffraction (XRD) techniques
  • Understanding of resolution functions in diffraction analysis
  • Knowledge of standard reference materials like LaB6, Si, and Al2O3
  • Experience with data fitting techniques in scientific analysis
NEXT STEPS
  • Research the concept of resolution functions in XRD analysis
  • Learn how to measure and analyze XRD patterns using the Rigaku SmartLab
  • Explore the process of fitting data to extract instrumental line broadening
  • Investigate the availability and application of NIST standard reference materials
USEFUL FOR

This discussion is beneficial for materials scientists, X-ray diffraction analysts, and researchers involved in precision measurements using the Rigaku SmartLab diffractometer.

yasir.ustb
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Hi every one!

I want to know the instrumental line broadening of Rigaku smartlab diffractrometer. I have searched out but i could not find any refrence. Please help me

Thanks and best regards
 
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You mean that I have to measured XRD pattern of material like LaB6, Si and Al2O3 with the sam e instrument. Then fit the resolution function. But what is resolution function? how can i get instrumental line broadning from fitting of resolution function?
 

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