Maximizing Safety and Accuracy in Titration: Tips for Volumetric Analysis

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Discussion Overview

The discussion centers around the practice of titration in chemistry practicals, specifically focusing on the method of mouth pipetting and its implications for safety and accuracy. Participants explore challenges faced during titration, potential shortcuts for determining titre values, and the broader context of safety practices in different regions.

Discussion Character

  • Debate/contested
  • Technical explanation
  • Conceptual clarification

Main Points Raised

  • One participant expresses difficulty in achieving an exact 20 mL titre value using mouth pipetting and seeks shortcuts.
  • Another participant explains that one should suck more than the required volume, then use a finger to close the pipette and let excess solution drop until the mark is reached.
  • Concerns are raised about the continued teaching of mouth pipetting, with one participant stating it is outdated and potentially dangerous.
  • Another participant counters that not all regions have access to safer alternatives, highlighting economic disparities in laboratory practices.
  • A participant suggests that knowing the titre value beforehand can help avoid dilution errors caused by residual water in the flask, sharing a personal strategy of adjusting the volume taken.
  • Further discussion emphasizes the risks associated with mouth pipetting, including potential health hazards, and questions the affordability of safety equipment in less affluent areas.

Areas of Agreement / Disagreement

Participants express disagreement regarding the safety and practicality of mouth pipetting, with some advocating for its discontinuation while others highlight economic constraints that prevent the adoption of safer methods. The discussion remains unresolved with multiple competing views on the topic.

Contextual Notes

Participants acknowledge that safety practices can vary significantly based on economic conditions, and there are unresolved issues regarding the availability of safer pipetting methods in different regions.

smart_worker
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guys today i have my chemistry practicals.i have to do titration.i have to suck the pipette with my mouth.it is a rule that everyone must use their mouth only.it is very difficult for me to suck in exact 20ml of the solution and pipette out.so i am not getting the exact titre value.are there any shortcuts to find the titre value.
 
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You don't "suck exactly 20 mL". You suck more, use your finger to close the pipette, then you let the excess to drop out till the pipette is filled exactly to the mark.
 
Utterly ridiculous that in 2014 people are still being taught to mouth pipette. I thought this practice was prohibited almost everywhere.
 
gravenewworld said:
Utterly ridiculous that in 2014 people are still being taught to mouth pipette. I thought this practice was prohibited almost everywhere.

Sorry to say that, but you are just showing your ignorance - not every part of the world is rich enough.
 
smart_worker said:
are there any shortcuts to find the titre value.

You can't decide the concentration of a solution while looking at it. And you are not allowed to do more than that. One shortcut is to get to know the titre value first!
In my case the error was always due to leftover distilled water in the flask. It diluted the pipetted solution and I purposely used to take 0.1mL less than the observed titre value. It worked well for me!
 
Borek said:
Sorry to say that, but you are just showing your ignorance - not every part of the world is rich enough.

Yup, so expensive :rolleyes:

http://www.sciencelabsupplies.com/Pipette_Filler_Red.html


If you can afford to do chemistry, afford chemicasl, afford to have a lab, and afford glassware you can afford minor safety items that can prevent major injuries. Hey mouth pipetting, what a great way to get hepatitis or oral acid/base burns!
 
You are still not understanding the reality - this kind of safety is considered a luxury in many places. When GDP per capita is 50 times lower than in US, $5 is a serious expense.

And - without getting into details - OP doesn't live in US.
 

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