What Metal is in the Unknown Sulfate Sample from the Precipitate Lab?

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    Ap chemistry Lab
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SUMMARY

The discussion focuses on identifying the metal in an unknown sulfate sample using a precipitate lab procedure. The participant mixed the sulfate powder with Barium Nitrate to precipitate Barium Sulfate and then used HCl to enhance particle size through flocculation. The key equation is XSO4 + Ba(NO3)2 --> XNO3 + BaSO4, where X represents the unknown metal. The participant has approximately 1 gram of sulfate powder and 24.88 mL of Barium Nitrate solution, which is critical for calculating the molar mass of the unknown metal using stoichiometry.

PREREQUISITES
  • Understanding of stoichiometry in chemical reactions
  • Familiarity with precipitate formation and flocculation techniques
  • Knowledge of Barium Nitrate and its role in sulfate precipitation
  • Basic laboratory skills for measuring mass and volume accurately
NEXT STEPS
  • Calculate the molar mass of the unknown metal using the mass of the original sulfate and the mass of the precipitate
  • Research the properties and reactions of common sulfate compounds
  • Explore methods for confirming the identity of metal ions in solution
  • Learn about the implications of using HCl in precipitate formation and its effects on metal ion solubility
USEFUL FOR

Chemistry students, laboratory technicians, and educators involved in analytical chemistry and precipitation reactions will benefit from this discussion.

sn1

Homework Statement


I have a percipitate lab.
We have an unknown sulfate powder that we mixed with water and then added Barium Nitrate in order to get the sulfate out of the mix. The entire sulfate, nitrate mixture was mixed with HCl to make the particles bigger and then it was heated for flocculation. I filtered out the percipitate and got it's mass, as well as the volume of the new nitrate solution. Right now the equation is looking like:

Homework Equations


XSO4 +Ba(NO3)2 --> XNO3 +BaSO4

The Attempt at a Solution


I was thinking of using mass percents
 
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Wouldn't hurt if you told us what for you want to use these mass percentages.

In other words: you have described the procedure, but you have not explained what was the aim of the experiment.
 
Sorry! I need to find what the unknown substance is.
 
Do you know the mass of the original sulfate powder? With that information and the mass of the precipitate, you can calculate the molar mass of element X by simple stoichiometry.
 
hilbert2 said:
Do you know the mass of the original sulfate powder? With that information and the mass of the precipitate, you can calculate the molar mass of element X by simple stoichiometry.
Yes I have the mass of the original sulfate powder. I tried my best to get it as close to 1gram as possible, and there is about 24.88mL of the barium nitrate (because its concentration level we calculated how much we needed in order to make the best possible reaction). We then added 1 mL of HCl, and heated it in order to make the precipitate particles as large as possible.

Your idea is what I thought should be done, but got a bit confused because so much is happening within the lab. Thank you!
 
Also note that there may be more than one metal ion for every sulfate ion in the original sample, as in ##Na_2 SO_4##.
 
Have you established which metal your unknown sample contains?
 

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