Where can I get voltammetry testing performed?

  • Thread starter Thread starter hobbs125
  • Start date Start date
  • Tags Tags
    Testing
Click For Summary

Discussion Overview

The discussion revolves around finding locations or methods for performing voltammetry testing, specifically cyclic voltammetry, on an electrochemical cell. Participants explore potential resources, equipment, and DIY approaches related to electrochemical testing.

Discussion Character

  • Exploratory, Technical explanation, Debate/contested

Main Points Raised

  • One participant suggests contacting the local State University Chemistry department for testing services, though they express doubt about non-students being accommodated.
  • Another participant proposes that the physics department might also be a viable option for voltage/current curve testing, indicating it could be done with standard equipment.
  • A participant inquires about the possibility of using a USB oscilloscope for testing, specifically to determine the total capacitance of an electrochemical capacitor.
  • Another participant expresses skepticism about using an oscilloscope for this purpose but suggests a low-cost setup using an operational amplifier (opamp) to maintain potential in the solution while measuring current.
  • One participant recommends contacting equipment manufacturers to see if they can perform the testing or know customers who could assist, emphasizing the complexity of constructing a potentiostat.
  • Another participant argues that while a simple potentiostat for cyclic voltammetry is not overly complex, some knowledge is required, and they suggest seeking permission from a nearby laboratory if unsure.
  • A participant notes the need for a potentiostat that can control potential, sweep rate, and measure small currents accurately, indicating that their approach differs from the previous suggestion of using an opamp, preferring to rely on more knowledgeable individuals.
  • One participant reiterates the complexity of building a potentiostat, mentioning that some standard commercial power supplies could be used, though they caution against the ease of cobbling together such equipment.

Areas of Agreement / Disagreement

Participants express differing views on the feasibility of constructing a potentiostat and the best resources for testing. There is no consensus on the optimal approach or location for performing the voltammetry testing.

Contextual Notes

Participants highlight the need for specific knowledge and equipment for effective voltammetry testing, indicating that the discussion is limited by varying levels of expertise and access to resources.

Who May Find This Useful

Individuals interested in electrochemistry, particularly those seeking practical advice on voltammetry testing methods and equipment options.

hobbs125
Messages
108
Reaction score
0
I have an electrochemical cell I need to get testing done on (namely cyclic voltammetry).

Problem is, I have no idea where to go?

Any suggestions?

I was thinking of contacting the local State University Chemistry department but I doubt it if they would do testing for someone who is not a student?
 
Chemistry news on Phys.org
Voltage/Current curves? I would ask the physics department, too, it looks like this could be done with standard equipment and not too much time.
 
Hmm, Is there anyway I could perform the tests using an oscilloscope?

I have a propscope (USB oscilloscope).

I am trying to determine the total capacitance (EDL and pseudo) of an electrochemical capacitor.
 
I doubt you can do it using Osciloscope. however you can make a small setup at low cost using opamp though. All you need to supply some voltage and receive the current while maintaining a potential into the solution using feedback. You need some idea though.
 
Find some equipment manufacturers and ask if they could perform the work or if they know if any of their customers could. Potentiostats are NOT trivial pieces of equipment that you can cobble together easily.
 
if you are not looking for too many functionality, yes a simple potentiostat able to do Cyclic voltammetry is NOT a rocket science...But as i said you need some idea ofcourse...if not better look for permission in a nearby laboratory
 
Hmmm, you need to construct a potentiostat that allows you to control potential, sweep rate and measure tiny currents accurately. I suppose it will need to be sized appropriately for the conductivity of the solution and surface area of the electrodes. I guess your idea of an opamp and mine are a bit different. I prefer to cause it to be done by others more knowledgeable than me.
 
chemisttree said:
Potentiostats are NOT trivial pieces of equipment that you can cobble together easily.
According to a quick google search, some standard commercial power supplies can be used for that. They are not cheap, but they can be found in many electronics labs. I don't want to advertise manufacturers, however.
 

Similar threads

  • · Replies 4 ·
Replies
4
Views
5K
  • · Replies 4 ·
Replies
4
Views
2K
  • · Replies 3 ·
Replies
3
Views
3K
Replies
12
Views
4K
  • · Replies 0 ·
Replies
0
Views
2K
  • · Replies 1 ·
Replies
1
Views
3K
  • · Replies 18 ·
Replies
18
Views
2K
  • · Replies 1 ·
Replies
1
Views
2K
  • · Replies 9 ·
Replies
9
Views
3K
  • · Replies 12 ·
Replies
12
Views
4K