Differential scanning calorimetry of nylon 6

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Quentin_alex
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Hello,

I ran a test on an industrial composite of 30% glass-filled nylon 6, and my melting temperature peak is too low. The range was from -30 C to 275 C. Why could this be happening? Should I suspect the sample pan?

Thanks.
 
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Quentin_alex said:
I ran a test on an industrial composite of 30% glass-filled nylon 6, and my melting temperature peak is too low. The range was from -30 C to 275 C. Why could this be happening? Should I suspect the sample pan?
What's the scan rate?