Differential scanning calorimetry of nylon 6

Hello,

I ran a test on an industrial composite of 30% glass-filled nylon 6, and my melting temperature peak is too low. The range was from -30 C to 275 C. Why could this be happening? Should I suspect the sample pan?

Thanks.
 

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I ran a test on an industrial composite of 30% glass-filled nylon 6, and my melting temperature peak is too low. The range was from -30 C to 275 C. Why could this be happening? Should I suspect the sample pan?
What's the scan rate?
 

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