Help me identify this mystery structure in my SEM image?

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SUMMARY

The discussion centers on identifying mysterious circular structures observed in scanning electron microscopy (SEM) images of a pyrex glass cell that contained a mixture of xenon and nitrogen gas, along with rubidium. The cell was subjected to 795 nm laser irradiation and temperatures up to 180°C. The user noted that these structures were absent in a control sample and speculated they could be surface defects resembling impact craters, potentially caused by microscopic impacts or xenon excimers. The inquiry seeks expert opinions on the nature of these features.

PREREQUISITES
  • Understanding of scanning electron microscopy (SEM) techniques
  • Familiarity with pyrex glass properties and behavior under irradiation
  • Knowledge of xenon excimer formation and its effects on materials
  • Experience with surface defect analysis in materials science
NEXT STEPS
  • Research the effects of xenon excimers on glass surfaces
  • Study the principles of scanning electron microscopy (SEM) imaging
  • Explore literature on microcratering phenomena in materials
  • Investigate methods for analyzing surface defects in glass
USEFUL FOR

This discussion is beneficial for materials scientists, researchers in semiconductor fabrication, and professionals involved in the analysis of surface defects in glass and other materials.

CFlower
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Hey all,

As the title suggests, I've found some recurring structure on an SEM image and I can't for the life of me figure out what it is. I took the image this morning.

Here she is:
http://i.imgur.com/nFuBsW2.png

Here's a larger, more zoomed out and higher res version. A few more of the mystery objects are visible.

http://i.imgur.com/gEXW4KN.jpg

I found plenty of these things. Here's some background on the sample. This was a piece of pyrex from a glass cell that contained a mixture of xenon and nitrogen gas. It also contained rubidium. The cell was continuously irradiated with 795 nm laser light, and heated sometimes up to 180 C. We washed out the rubidium by slowly reacting it with alcohol before breaking the cell open. I've been examining the cell surface looking for etching or pitting in the glass possibly caused by xenon excimers. So far, inconclusive. But I've been completely baffled by these circular structures that keep appearing. They were not present at all on a control piece of pyrex that I imaged.

Does anyone recognize this? What might it be?

Thanks!
 
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I am not familiar with scanning electron microscopy, but the features look very similar to impact craters. Especially since they all seem to contain some central feature. Perhaps it is a surface defect due to microscopic impacts.
 

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