How can i stick metal nanoparticles on glass?

In summary, the conversation discusses methods for characterizing metallic nanoparticles with SEM. The individual has tried depositing them on a glass substrate, but it did not work. They are seeking help or suggestions for an appropriate solution. It is suggested that knowing the concentration of the nanoparticles and using TEM or AFM may be better options, as glass is an insulator and may not work well with SEM. The LBL method is also mentioned as a potential solution.
  • #1
nadaben
14
0
to caracterize for exple metallic nanoparticles with SEM i should deposite them on a substrate
i tried a deposition on glass substrate but it doesn't work and i see nothing
can anyone help me or suggest an appropriate solution to that
best regards
 
Chemistry news on Phys.org
  • #2
Your previous posts have indicated you're trying to make colloidal gold. Do you know the concentration of nanoparticles in your solution? If your solution is concentrated enough to be colored, you should be able to just dropcast NPs onto a glass slide. But for SEM, glass is a bad idea: it's an insulator, so it'll charge like crazy. There are ways to do non-conductive SEM, but I'm not too familiar with them (I think they involve low voltages = lower resolution). TEM might be a better option, as the structures you're looking for will probably be less than 100 nm. AFM is another option, but it can be challenging differentiating between nanoparticles and ordinary dirt.
 
  • #3
Actually my solution is not that much concentrated when i deposit a drop it's almost colorless
thank you for other informations it's very interesting
 
  • #4
Have you tried layer-by-layer (LBL) method? See references by Kotov, et. al.
 

1. How do metal nanoparticles stick to glass?

Metal nanoparticles can stick to glass through a process called functionalization, where the surface of the glass is treated with a chemical compound that allows the nanoparticles to bind to it. This can be achieved through methods such as silanization or thiolation, which create chemical bonds between the glass surface and the nanoparticles.

2. What types of metal nanoparticles can be used for sticking to glass?

Various types of metal nanoparticles can be used for sticking to glass, such as gold, silver, platinum, and titanium nanoparticles. The type of metal used will depend on the specific application and properties desired.

3. Can metal nanoparticles be directly applied to glass without any treatment?

No, metal nanoparticles cannot be directly applied to glass without any treatment. Glass surfaces are typically hydrophilic, meaning they have a high affinity for water molecules and do not interact well with hydrophobic metal nanoparticles. Thus, the surface must be modified in order for the nanoparticles to adhere to it.

4. How can the stability of metal nanoparticles on glass be improved?

The stability of metal nanoparticles on glass can be improved by using stabilizing agents, such as surfactants or polymers, that prevent the nanoparticles from agglomerating or falling off the surface. Additionally, controlling the size and shape of the nanoparticles can also improve their stability on the glass surface.

5. Are there any limitations to using metal nanoparticles on glass?

There are some limitations to using metal nanoparticles on glass, such as the potential for toxicity and environmental concerns. Additionally, factors such as the glass composition and surface roughness can affect the stability and adhesion of the nanoparticles. It is important to consider these limitations and select the appropriate metal nanoparticles and functionalization methods for each specific application.

Similar threads

Replies
12
Views
1K
Replies
5
Views
1K
Replies
16
Views
2K
Replies
3
Views
1K
  • General Engineering
Replies
10
Views
239
Replies
2
Views
2K
Replies
6
Views
1K
  • Materials and Chemical Engineering
Replies
1
Views
2K
Back
Top