How can i stick metal nanoparticles on glass?

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Discussion Overview

The discussion revolves around the challenges of depositing metal nanoparticles onto glass substrates for characterization, particularly using scanning electron microscopy (SEM). Participants explore various methods and considerations related to the deposition process and the suitability of different techniques for imaging nanoparticles.

Discussion Character

  • Exploratory
  • Technical explanation
  • Debate/contested

Main Points Raised

  • One participant notes difficulties in depositing metallic nanoparticles on glass substrates for SEM characterization, seeking assistance.
  • Another participant suggests that the concentration of nanoparticles in the solution may affect visibility and mentions that glass is an insulator, which can lead to charging issues during SEM imaging.
  • A different participant indicates that their solution is not concentrated enough, resulting in a colorless drop when deposited.
  • One participant proposes the layer-by-layer (LBL) method as a potential solution, referencing work by Kotov et al.

Areas of Agreement / Disagreement

Participants express differing views on the effectiveness of glass as a substrate for SEM and the concentration of nanoparticles necessary for successful deposition. The discussion remains unresolved regarding the best method for deposition and characterization.

Contextual Notes

Participants have not reached consensus on the optimal substrate or method for depositing nanoparticles, and there are unresolved questions regarding the concentration of nanoparticles needed for effective imaging.

nadaben
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to caracterize for exple metallic nanoparticles with SEM i should deposite them on a substrate
i tried a deposition on glass substrate but it doesn't work and i see nothing
can anyone help me or suggest an appropriate solution to that
best regards
 
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Your previous posts have indicated you're trying to make colloidal gold. Do you know the concentration of nanoparticles in your solution? If your solution is concentrated enough to be colored, you should be able to just dropcast NPs onto a glass slide. But for SEM, glass is a bad idea: it's an insulator, so it'll charge like crazy. There are ways to do non-conductive SEM, but I'm not too familiar with them (I think they involve low voltages = lower resolution). TEM might be a better option, as the structures you're looking for will probably be less than 100 nm. AFM is another option, but it can be challenging differentiating between nanoparticles and ordinary dirt.
 
Actually my solution is not that much concentrated when i deposit a drop it's almost colorless
thank you for other informations it's very interesting
 
Have you tried layer-by-layer (LBL) method? See references by Kotov, et. al.
 

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