I was trying to brief earlier. The first two paragraphs only talk about the start of the experiment and the lower layer. Reading the third will probably clarify everything.
Benzoic acid/biphenyl mixture was a white powdery solid. It was 2.08g. It was dissolved in 30mL of diethyl ether in an...
The issue is, when I do Percent recovery right away. I get crazy answers. (0.9[benzoic acid] + 27.11[biphenyl])/2.08 x 100 = 1346 %
Mass of RBF + boiling stones= 61.61g
Mass of RBF + bioling stones + biphenyl = 88.72g
Mass of biphenyl = 27.11g
The biphenyl itself was very little in substance...
I've been trying to convert the benzoic acid/biphenyl to moles to find the limiting reactant, then comparing the number of moles in order to find percent recovery. But I cannot get the equation or the mass used to find theoretical yield since there is only one mass (2.08 g)
The mass of the benzoic acid/biphenyl mixture was 2.08 g.
Biphenyl product was placed in a pre-weighed round bottom flask. I didn't take the measurement for the pre-weighed stuff, it was copied from a partner. Pre-weighed rbf was 61.61g. When I weighed it after leaving it alone, it was 88.72g...
Homework Statement
Benzoic acid/biphenyl mixture is mixed with diethyl ethe(CH3CH2-O-CH2CH3). The solution is placed in a separatory funnel and sodium hydroxide is mixed in.
The bottom layer, H2O, NaOH and benzoic acid is then placed in a flask where it is mixed with HCl, chilled and then...
Homework Statement
Compound A
mass - 11.0g
solubility in ethanol at 78 deg C - 0.53 g/mL
solubility in ethanol at 0 deg C - 0.08 g/mL
Impurity B
mass - 2.5 g
solubility in ethanol at 78 deg C - 0.82 g/mL
solubility in ethanol at 0 deg C - 0.12 g/mL
Impurity C
mass - 2.5 g
solubility in...