Experimenting with a vacuum pump

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Discussion Overview

The discussion revolves around the safe operation of a vacuum pump and bell jar setup for experiments. Participants seek guidance on the correct sequence for switching off the pump and safely dismantling the experimental setup, addressing concerns about potential damage to the pump and the bell jar.

Discussion Character

  • Exploratory
  • Technical explanation
  • Debate/contested
  • Experimental/applied

Main Points Raised

  • One participant inquires about the procedure for switching off the vacuum pump after evacuating the bell jar, expressing concerns about potential damage to the pump or oil being sucked out.
  • Another participant suggests that it is likely fine to switch off the pump while monitoring the vacuum gauge for leaks and recommends using a bleed valve to return to atmospheric pressure.
  • Some participants mention the importance of having a valve at the pump to reduce leakage and the necessity of another valve to let air back into the chamber.
  • Participants discuss a proposed sequence for safely dismantling the setup, including closing the valve between the pump and bell jar before switching off the pump.
  • Concerns are raised about the strength of the bell jar and the need to ensure it is rated for vacuum use.
  • One participant shares their positive experience using a school vacuum pump for similar experiments, emphasizing the importance of a sealing valve.
  • Another participant notes the use of a safe plastic bell jar and mentions the successful execution of the proposed procedure.

Areas of Agreement / Disagreement

Participants express a range of views on the procedure for safely operating the vacuum pump and bell jar. While some agree on the proposed steps, others raise concerns about potential risks, indicating that the discussion remains unresolved regarding the safest approach.

Contextual Notes

Participants have not reached a consensus on the best practices for operating the vacuum pump and bell jar, and there are varying opinions on the necessity of additional valves and the strength of the bell jar.

DDesulgon
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Hello,
I would like to carry out a few experiments with a vacuum pump under a vacuum bell jar. However, I have no experience with this and the operating instructions could only help me to a limited extent.
Specifically, I am interested in the sequence for switching off the pump: When I have pumped the air out of the bell jar, can I then simply switch off the pump? Or will the vacuum in the bell jar damage the pump or suck the oil out of it or something similar?
What are the next steps when dismantling the experiment? Let air back into the bell, pull off the pump hose... In what order should one proceed?
 
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Can you post links to the pump and bell jar info? Most likely it's fine to switch off the pump and just watch the vacuum gauge to be sure you don't have a leak, and then just crack the bleed valve when you are ready to return it back to atmospheric pressure, but it would be good to see the pump and bell jar info to be sure.

1652106481198.png

https://www.spectrum-scientifics.com/High-Vacuum-Pump-Deluxe-Experiment-Kit-p/1907.htm
 
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It is common for there to be a valve at the pump to reduce the leakage back through the pump (which should be small). It may not be necessary if you don't need a hard vacuum or you don't need to maintain it for a really long time. You'll also need another valve to let air back into the chamber at some point.
 
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Thanks for the answers and the link! Unfortunately I cannot find the information about the pump and the bell jar online.
Do I understand it correctly that the following way is safe?
- Pump off air
- Close the valve between the pump and the bell jar
- Switch off pump
- Remove the hose from valve
- open valve to let air back into the chamber (I have only the one valve)
Or could something still potentially go wrong with this procedure? And if so, what would be an alternative approach?
 
DDesulgon said:
Hello,
I would like to carry out a few experiments with a vacuum pump under a vacuum bell jar. However, I have no experience with this and the operating instructions could only help me to a limited extent.
Specifically, I am interested in the sequence for switching off the pump: When I have pumped the air out of the bell jar, can I then simply switch off the pump? Or will the vacuum in the bell jar damage the pump or suck the oil out of it or something similar?
What are the next steps when dismantling the experiment? Let air back into the bell, pull off the pump hose... In what order should one proceed?
What kind of experiments are you wanting to do if I may ask?
 
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DDesulgon said:
Thanks for the answers and the link! Unfortunately I cannot find the information about the pump and the bell jar online.
Do I understand it correctly that the following way is safe?
- Pump off air
- Close the valve between the pump and the bell jar
- Switch off pump
- Remove the hose from valve
- open valve to let air back into the chamber (I have only the one valve)
Or could something still potentially go wrong with this procedure? And if so, what would be an alternative approach?

I would do something like this:

Bell Jar.jpg


The ball valve should be vacuum rated, and I believe a "T port".
 
Last edited:
DDesulgon said:
Thanks for the answers and the link! Unfortunately I cannot find the information about the pump and the bell jar online.
Do I understand it correctly that the following way is safe?
- Pump off air
- Close the valve between the pump and the bell jar
- Switch off pump
- Remove the hose from valve
- open valve to let air back into the chamber (I have only the one valve)
Or could something still potentially go wrong with this procedure? And if so, what would be an alternative approach?
Sounds good to me. The only thing I'd worry about is the bell jar strength; but it will be fine if it's intended for vacuum use.
 
DaveE said:
Sounds good to me. The only thing I'd worry about is the bell jar strength; but it will be fine if it's intended for vacuum use.
Just wear safety glasses.
 
  • #10
I have used a safe plastic bell jar made by Nalgene, but expensive.
 
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  • #11
I did it as described above and it worked nicely. Thank you all for the quick and excellent help, as always.
 
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