Molecular Seive for making vacuum tubes

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SUMMARY

The discussion centers on the use of molecular sieves in vacuum tube manufacturing, specifically employing zeolites for moisture removal during the roughing process. The participant recalls utilizing a molecular sieve canister cooled with liquid nitrogen to achieve pressures around 10 microns. The primary function of the sieve is to adsorb water molecules, although it can also adsorb nitrogen at low temperatures. The sequence of operations includes using a mechanical pump to 10 microns, isolating the system, employing the molecular sieve, and finally using a vacuum ion pump to reach pressures as low as 10-14 torr, crucial for maintaining cathode properties in vacuum tubes.

PREREQUISITES
  • Understanding of vacuum systems and their components
  • Knowledge of molecular sieves and zeolite materials
  • Familiarity with vacuum pressure measurements (torr and microns)
  • Experience with vacuum ion pumps and their operation
NEXT STEPS
  • Research the properties and applications of zeolites in vacuum technology
  • Learn about the operation and maintenance of mechanical pumps for vacuum systems
  • Explore the principles of adsorption processes in vacuum applications
  • Investigate the effects of oil contamination on vacuum tube performance
USEFUL FOR

Engineers, vacuum technology specialists, and professionals involved in the manufacturing and maintenance of vacuum tubes will benefit from this discussion.

Y2keddie
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im trying to jog my memory back 30years when I worked with vacuum tubes. I worked with manufacturing of image tubes. I remember the vacuum systems used vac-ion pumps to achieve -12 power torr. I alsoo remember first using a molecular seive for roughing,pumping to 10 microns.
The seive was a canister filled with a zeonolite which was cooled with liquid nitrogen.
I believe it worked as an adosorbtion process where water molecules would adhere to the zenolite surface thus removing water molecules from air in the beginning stages of vacuum.
What my memory is fuzzy about: is the seive used just for water,or other gas molecules?
 
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My recall is not that good. I’m guessing the process sequence was:

Use Mechanical pump ( to 10 microns).
Isolate
Then molecular Seive (to ?? Torr) The decrease in pressure would indicate the oil molecules had decreased?
Isolate
Then Vac Ion pump to 10x-14 torr

That would make sense. The oil contaminants would destroy the tubes cathode properties.
 
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