Ultra high vacuum with scanning tunneling microscope

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Discussion Overview

The discussion centers on the requirements and considerations for building an ultra high vacuum (UHV) chamber for use with a scanning tunneling microscope (STM), particularly in the context of moving atoms. Participants seek and provide information on the necessary equipment, techniques, and challenges involved in such projects.

Discussion Character

  • Technical explanation
  • Exploratory
  • Debate/contested

Main Points Raised

  • One participant requests general information about UHV and STM, including temperature requirements and types of pumps needed.
  • Another participant suggests that the need for UHV is independent of the specific application and emphasizes the importance of learning from existing systems or experienced individuals.
  • A detailed response outlines the necessary equipment, including an oiless roughing pump, turbo pump, and either an ion pump or cryopump, along with vacuum gauges for measuring low pressures.
  • Concerns are raised about the complexity of designing the vacuum system and the importance of maintaining "UHV hygiene" through proper cleaning techniques and materials.
  • One participant warns that building a UHV device requires experienced guidance and significant financial investment, suggesting that it may take years to develop the capability to manipulate atoms with an STM.

Areas of Agreement / Disagreement

Participants express varying levels of agreement on the necessity of experienced guidance and the financial implications of building a UHV system. There is no consensus on the feasibility of undertaking such a project without prior experience or support.

Contextual Notes

Limitations include the lack of specific details on the design process and the potential variations in equipment and techniques based on individual project needs. The discussion does not resolve the complexities involved in achieving UHV or the specific requirements for STM operation.

baconbits423
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I am working on a project involving a scanning tunneling microscope, and to move atoms i need an untra high vacuum chamber. Any info you have on UHV or STM would be immensly appreciated.:rolleyes:




Thanks
 
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baconbits423 said:
I am working on a project involving a scanning tunneling microscope, and to move atoms i need an untra high vacuum chamber. Any info you have on UHV or STM would be immensly appreciated.:rolleyes:

What kind of information do you need? As in what type of pumps and gauges to use?

Zz.
 
:rolleyes: Any thing, mostly about a uhv, for example does it need to be at a certain temp, what types of pumps are needed, what is necessary to use a scanning tunneling microscope to lift atoms off of a surface.
 
baconbits423 said:
:rolleyes: Any thing, mostly about a uhv, for example does it need to be at a certain temp, what types of pumps are needed, what is necessary to use a scanning tunneling microscope to lift atoms off of a surface.

It has nothing to do with the uses. If you need UHV, then the technique is similar no matter what it is used for.

I gather that you don't have any other persons around that can help you with this? Usually, in many cases, people learn from existing systems, or from people who have either assembled or maintained such a system. So asking something like this from ground zero is rather unusual.

You definitely need (i) an oiless roughing pump (ii) a turbo pump and (iii) either an ion pump or a cryopump. The roughing pump will serve 2 purposes: (i) to get you to approximately 10^-5 Torr and then you can start the turbo pump and (ii) to back your turbo pump. Once you get to low 10^-7, then you can start the ion/cryopump.

You will also need one regular vacuum gauge and an ion gauge that can go to 10^-12 torr.

The most tedious part is designing where such pumps should go. You want to minimize the use of vacuum lines because this will only reduce the conductance and lower your pumping efficiency. You will also need to learn "UHV hygene". Cleaning the parts that go into the system is essential (one usually clean them with citrinox solution in an ultrasound bath, and then acetone+ethanol rinse), and vacuum-approved gloves and wiping cloth and aluminum foil are also required.

Again, it is difficult to describe the process on here if you want to have a complete picture. I strongly suggest you find someone who has done this, and who has a good "vacuum" technique.

Zz.
 
You cannot build an UHV device if you do not have experienced people besides you to guide and help you. You cannot build it for less than several thousand dollars (or tens of thousands).
For the TSM the situation is very similar. If you are an experienced physicist with a good knowledge in electronics and a good funding you can (may be) built it in a year. To be able to move atoms, you can add a few more years.
 

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