Any idea how to bake the column of a SEM?

Click For Summary
SUMMARY

The discussion centers on the process of baking the column and gun chamber of a Scanning Electron Microscope (SEM) donated by DOW Chemical. The user seeks guidance on this procedure after receiving a costly quote of $17,000 from the company for professional assistance. They share their previous experience using heater tape, a resistive wire tape that generates heat when current is applied, to bake out vacuum systems. The recommended method involves wrapping the heater tape around the vacuum chamber and applying a vacuum while heating to eliminate volatile contaminants.

PREREQUISITES
  • Understanding of Scanning Electron Microscopes (SEM)
  • Familiarity with vacuum systems
  • Knowledge of heater tape and its applications
  • Basic electrical safety and handling
NEXT STEPS
  • Research the specifications and proper usage of heater tape for vacuum applications
  • Learn about the vacuum pumping process and its importance in SEM maintenance
  • Investigate best practices for cleaning and maintaining SEM components
  • Explore alternative methods for baking out vacuum systems
USEFUL FOR

Undergraduate researchers, laboratory technicians, and anyone involved in the maintenance and operation of Scanning Electron Microscopes.

Old_Bob
Messages
2
Reaction score
0
I am an undergraduate researcher and my university had an SEM donated to us by DOW chemical. It since has been without power and we have to bake the column and the gun chamber. Contacting the company they estimate $17k to send someone out to do it for us. I'm having difficulty finding material online for how to do this. Does anyone know how?
 
Engineering news on Phys.org
In my past experience we baked out vacuum systems by wrapping them with heater tape. This is a metallic tape with a resistive wire inside that heats up when you pass current through it. If you google "heater tape" you will find several sources. You wrap the heater tape around the vacuum chamber and then pump on it while you heat it up to drive off volatile contaminants.
 
  • Like
Likes   Reactions: Old_Bob
Thank you! I'll look into it
 

Similar threads

Replies
8
Views
5K
Replies
1
Views
3K
Replies
4
Views
4K
  • · Replies 4 ·
Replies
4
Views
7K
  • · Replies 3 ·
Replies
3
Views
4K
  • · Replies 80 ·
3
Replies
80
Views
69K
  • · Replies 11 ·
Replies
11
Views
9K
  • · Replies 5 ·
Replies
5
Views
3K
  • · Replies 5 ·
Replies
5
Views
3K
  • Sticky
  • · Replies 2 ·
Replies
2
Views
506K