In my attempt at standardizing an EDTA solution, the blank solution titration was successful, but the standardization titration failed... here's the procedure of my experiment with some details: We first prepared a titration blank by using 35mL distilled water, 5mL of pH10 buffer, 5 drops of Eriochrome Black T indicator, which made a black solution. We then added 15 drops of 0.03M magnesium chloride to the solution, which turned it red. We titrated this using an unknown concentration of EDTA solution. The next part of the experiment involved using 0.2-0.3g of calcium carbonate (dissolved with 1 mL 3M HCl and 4 mL DI water). We mixed this solution with the indicator solution prepared in the titration of the blank. We titrated this solution using EDTA, expecting somewhere between 30-50 mL to be needed. We went over 80 mL in 3 consecutive trials, and never ended up reaching the endpoint of the titration. Any ideas as to where our experiment could have gone wrong? Thanks!