Experimenting with a vacuum pump

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SUMMARY

This discussion focuses on the safe operation of a vacuum pump in conjunction with a vacuum bell jar for experimental purposes. Key steps include pumping air out, closing the valve between the pump and the bell jar, switching off the pump, and then allowing air back into the chamber. The use of a vacuum-rated ball valve is recommended to prevent backflow and ensure safety. Participants confirm that using a properly rated bell jar, such as those from Nalgene, is crucial for maintaining structural integrity during experiments.

PREREQUISITES
  • Understanding of vacuum systems and their components
  • Familiarity with vacuum-rated valves, specifically ball valves
  • Knowledge of safety protocols when working with vacuum equipment
  • Experience with vacuum pumps, particularly school or laboratory-grade models
NEXT STEPS
  • Research the specifications and safety features of Nalgene vacuum bell jars
  • Learn about the operation and maintenance of high vacuum pumps
  • Explore the use of vacuum-rated ball valves in experimental setups
  • Investigate best practices for safely dismantling vacuum experiments
USEFUL FOR

This discussion is beneficial for educators, students conducting physics experiments, and hobbyists interested in vacuum technology and safety procedures when using vacuum pumps and bell jars.

DDesulgon
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Hello,
I would like to carry out a few experiments with a vacuum pump under a vacuum bell jar. However, I have no experience with this and the operating instructions could only help me to a limited extent.
Specifically, I am interested in the sequence for switching off the pump: When I have pumped the air out of the bell jar, can I then simply switch off the pump? Or will the vacuum in the bell jar damage the pump or suck the oil out of it or something similar?
What are the next steps when dismantling the experiment? Let air back into the bell, pull off the pump hose... In what order should one proceed?
 
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Can you post links to the pump and bell jar info? Most likely it's fine to switch off the pump and just watch the vacuum gauge to be sure you don't have a leak, and then just crack the bleed valve when you are ready to return it back to atmospheric pressure, but it would be good to see the pump and bell jar info to be sure.

1652106481198.png

https://www.spectrum-scientifics.com/High-Vacuum-Pump-Deluxe-Experiment-Kit-p/1907.htm
 
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It is common for there to be a valve at the pump to reduce the leakage back through the pump (which should be small). It may not be necessary if you don't need a hard vacuum or you don't need to maintain it for a really long time. You'll also need another valve to let air back into the chamber at some point.
 
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Thanks for the answers and the link! Unfortunately I cannot find the information about the pump and the bell jar online.
Do I understand it correctly that the following way is safe?
- Pump off air
- Close the valve between the pump and the bell jar
- Switch off pump
- Remove the hose from valve
- open valve to let air back into the chamber (I have only the one valve)
Or could something still potentially go wrong with this procedure? And if so, what would be an alternative approach?
 
DDesulgon said:
Hello,
I would like to carry out a few experiments with a vacuum pump under a vacuum bell jar. However, I have no experience with this and the operating instructions could only help me to a limited extent.
Specifically, I am interested in the sequence for switching off the pump: When I have pumped the air out of the bell jar, can I then simply switch off the pump? Or will the vacuum in the bell jar damage the pump or suck the oil out of it or something similar?
What are the next steps when dismantling the experiment? Let air back into the bell, pull off the pump hose... In what order should one proceed?
What kind of experiments are you wanting to do if I may ask?
 
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DDesulgon said:
Thanks for the answers and the link! Unfortunately I cannot find the information about the pump and the bell jar online.
Do I understand it correctly that the following way is safe?
- Pump off air
- Close the valve between the pump and the bell jar
- Switch off pump
- Remove the hose from valve
- open valve to let air back into the chamber (I have only the one valve)
Or could something still potentially go wrong with this procedure? And if so, what would be an alternative approach?

I would do something like this:

Bell Jar.jpg


The ball valve should be vacuum rated, and I believe a "T port".
 
Last edited:
DDesulgon said:
Thanks for the answers and the link! Unfortunately I cannot find the information about the pump and the bell jar online.
Do I understand it correctly that the following way is safe?
- Pump off air
- Close the valve between the pump and the bell jar
- Switch off pump
- Remove the hose from valve
- open valve to let air back into the chamber (I have only the one valve)
Or could something still potentially go wrong with this procedure? And if so, what would be an alternative approach?
Sounds good to me. The only thing I'd worry about is the bell jar strength; but it will be fine if it's intended for vacuum use.
 
DaveE said:
Sounds good to me. The only thing I'd worry about is the bell jar strength; but it will be fine if it's intended for vacuum use.
Just wear safety glasses.
 
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I have used a safe plastic bell jar made by Nalgene, but expensive.
 
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  • #11
I did it as described above and it worked nicely. Thank you all for the quick and excellent help, as always.
 
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