Question about an experiment to make carbon boride

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SUMMARY

The discussion centers on the creation of carbon boride using a homemade reaction chamber from an old propane tank. The user intends to achieve the necessary reaction temperatures by applying a DC current. Key considerations include whether to fill the chamber with argon or to create a vacuum, with specific inquiries about the required vacuum levels for safety and efficacy. The user expresses concerns regarding the safety of the experiment, indicating a need for caution.

PREREQUISITES
  • Understanding of chemical reactions involving carbon and boron.
  • Knowledge of high-temperature reaction environments.
  • Familiarity with gas atmospheres in chemical processes, specifically argon.
  • Experience with vacuum systems and their operational parameters.
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  • Research the properties and synthesis methods of carbon boride.
  • Learn about the design and safety protocols for homemade reaction chambers.
  • Investigate the requirements for creating and maintaining a vacuum chamber.
  • Explore the use of argon in high-temperature chemical reactions.
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Chemists, materials scientists, and hobbyists interested in experimental synthesis of advanced materials, particularly those working with high-temperature reactions and vacuum systems.

Warpspeed13
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Ok what kind of environment do I have to create for the reaction to take place? I'm turning an old propane tank into a reaction chamber and to achieve the temperatures required for reaction I will run a DC current through the material. Will filling the chamber with argon be sufficient or does it need to be a vacuum chamber? If so how much of a vacuum is necessary?
 
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I am not convinced it is a safe enough experiment to be discussed here.

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