Reciprocal Lattice: Visible Points in an X-Ray Experiment

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SUMMARY

The discussion focuses on the visibility of reciprocal lattice points in X-ray diffraction experiments. It is established that only specific reciprocal lattice points corresponding to parallel planes become visible based on the orientation of the incident beam. To observe different reciprocal points, one must change the orientation of the beam to involve other sets of parallel planes. The phenomenon can also allow for multiple reflections under certain conditions, known as the Renninger effect or multiple beam diffraction, which can be achieved by adjusting the azimuthal angle and photon energy.

PREREQUISITES
  • Understanding of reciprocal lattice concepts
  • Familiarity with X-ray diffraction principles
  • Knowledge of Bragg's law and conditions for diffraction
  • Experience with crystal orientation techniques in diffraction experiments
NEXT STEPS
  • Research the Renninger effect in X-ray diffraction
  • Learn about multiple beam diffraction techniques
  • Study the application of Ewald's sphere in reciprocal space
  • Explore the use of computer codes for calculating Umwegs in diffraction
USEFUL FOR

Researchers in materials science, physicists studying crystallography, and anyone involved in X-ray diffraction experiments will benefit from this discussion.

Dr_Pill
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I got a bunch of questions about reciprocal lattice, I start with this one:

In an x-ray experiment:

For one specific orientation of your incident beam on your real lattice, only a portion of the points of your reciprocal lattice will become visible as your diffraction pattern right?

See my picture

nm4bBeB.jpg


For one incident beam, only the parallel planes are involved in your diffraction and so only the reciprocal lattice points that represent these set of parallel planes will becoem visible on your diffraction pattern

If you want to make other reciprocal points points visible on your diffraction pattern, u have to change the orientation of your incident beam so that another set of parallel planes is involved in diffraction
So in first picture, your blue beam will get the reciprocal points that representing the green parallel planes visible on your diffraction pattern.

Second picture, the same blue beam does nothing on the purple planes, so the reciprocal points that represents the purple planes will not be visible on the diffraction pattern.

Is this correct?
 
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It might help with the Forum formatting if you reduce the size of your image to no more than 800 pixels by 600 pixels. There's no reason for it to be THIS big.

Zz.
 
ZapperZ said:
It might help with the Forum formatting if you reduce the size of your image to no more than 800 pixels by 600 pixels. There's no reason for it to be THIS big.

Zz.

Ok, like this? But now my picture is unsharp.
 
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Dr_Pill said:
how can i resize it?

Remove the image, and upload a new, resized version.

Zz.
 
Dr. Pill,

your images are in real space, not reciprocal space.

It is perfectly possible to align a single crystal such that two or even three sets of lattice planes fulfull the Bragg condition simultaneously.

For the two-beam case this can be done by aligning one Bragg peak (corresponding to the reciprocal space vector Q), and by then rotating the crystal about the vector Q until you excite a second reflection (=changing the azimuthal angle). To get 3 simultaneous reflections you also need to tune the photon energy just right.

The effect is known by several names including "Umweganregung", "Renninger effect" and "Multiple beam diffracton". It was first described in 1935.

The following links give a bit more informaiton:

P. P. Ewald, Rev. Mod. Phys. v37, pp46 (1965)
http://rmp.aps.org/abstract/RMP/v37/i1/p46_1
This is an excellent review article about the early theory of x-ray diffraction, written by one of the founding fathers. Highly recommended if you are interested in x-rays.

Renninger, Z. Phys v. 106 pp 141 (1937) in German
http://link.springer.com/article/10.1007/BF01340315

Description of a computer code for calculating Umwegs.
http://www1.uni-hamburg.de/mpi/rossmanith/Reprints/Z_Krist_85.pdf
 
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