OK, I took my sample into my brother's lab to test its density.We measured its volume by dropping it in a full beaker of water and measuring the weight (and thus volume) of the water that was displaced on a microgram scale. By far the biggest problems we had were:
- eliminating the meniscus so we cold get an accurate water level, and
- ensuring that we drained all drops from the exteroir of the beaker onto the weight scale.
We used combinations of alcohol and/or hand soap to minimize the meniscus and used a microlitre pipette to recover any drops that lingered on the beaker. My brother, having spent decades in the lab, was able to estimate the few microlitre drops remaining and added them to the test sample. We figure we got our volume measurements to within +/-20 microlitres. We did the experiment 3 times.
Results:
The sample weighs 116.06g.
The volume is 10.13, 10.56 and 10.64 cm^3 for an average of 10.44 cm^3.
This results in a density of 11.12g/cm^3 +/- 0.02.
The published density of common lead is 11.34g/cm^3.
My measurement of the sample is within 2% of the density of lead.
I'm callin' it lead.