Electron Diffraction: Calculate Crystal Plane Spacing

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SUMMARY

The discussion focuses on calculating the crystal plane spacing using electron diffraction, specifically with a beam of electrons at 50 eV kinetic energy. Bright rings are observed at angles of 20 degrees and 40.7 degrees, leading to the application of Bragg's law, represented by the equation 2d sin(theta) = n lambda. The user initially encounters discrepancies in calculated values of d due to assumptions about the order of maxima but resolves this by adjusting the angles before applying the formula, resulting in consistent values for d.

PREREQUISITES
  • Understanding of Bragg's Law in crystallography
  • Familiarity with the concepts of electron diffraction
  • Knowledge of kinetic energy and its relation to wavelength
  • Basic proficiency in algebra and trigonometry
NEXT STEPS
  • Study the derivation and applications of Bragg's Law in crystallography
  • Learn about the relationship between kinetic energy and wavelength in electron beams
  • Explore advanced topics in electron diffraction techniques
  • Investigate methods for minimizing discrepancies in experimental data analysis
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Students and researchers in physics, particularly those focusing on crystallography and materials science, as well as anyone interested in the practical applications of electron diffraction in determining crystal structures.

throneoo
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Homework Statement


a beam of electrons with a kinetic energy of 50eV is incident on a powdered crystal sample. A series of bright and dark rings is observed on a screen behind the sample, as shown below (a picture which shows two concentric circles with the beam passing through the center . ) If bright rings are observed at angles of theta =20 degrees and theta =40.7 degrees to the beam direction , calculate the spacing of the planes of the crystal.

Homework Equations


bragg diffraction , p=h/lambda ,E=p^2/2m

The Attempt at a Solution


I can find the wavelength using a combination of the 2nd and 3rd equation (E=(h/lambda)^2 / 2m )

but since no further information is given regarding the order of the bright fringes at those 2 angles (e.g. the relationship between the two maxima , in which order they are in etc.) I assumed they correspond to the 1st and 2nd maxima .
using 2d sin theta=n lambda , I can get two different values of d with the two angles .

However , the discrepancy between the two values is quite huge (about 10%) . therefore I don't know how to get a consistent value .

so I decided to find two integers n and m such that n/m is approximately equal to the ratio of the sines of the angles ~ 1.906608182 (which is just from the formula) , and minimize the discrepancy of d .

but I'm afraid I would get large values of n and m just to satisfy the condition , so large they are not even physically feasible .
 
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just realized I need to divide the angle by 2 before applying the formula . the values are much more consistent now .
 

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