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Discussion Overview

The discussion revolves around the search for a suitable spectrometer for investigating reaction kinetics in a lab setting. Participants explore various options, considerations for purchasing, and implications of laboratory setup.

Discussion Character

  • Exploratory
  • Technical explanation
  • Debate/contested

Main Points Raised

  • One participant is looking for a data logging spectrometer that maintains a constant temperature for reaction kinetics, with a budget of a couple thousand dollars.
  • Another participant inquires about the educational background and location of the lab, emphasizing the importance of adhering to regulations regarding chemical disposal and maintenance.
  • A suggestion is made that NMR could be a viable method for reaction kinetics if the reaction rate aligns with the NMR time scale, while noting that ReactIR may be too expensive for the stated budget.
  • A link to a directory of spectrometers is provided, with a comment that the original poster should research available options themselves.

Areas of Agreement / Disagreement

Participants express varying opinions on the best spectrometer options and methods for reaction kinetics, with no consensus reached on specific models or approaches.

Contextual Notes

There are unresolved questions regarding the legality and regulations of laboratory practices, as well as the compatibility of different spectrometer types with the intended experiments.

Who May Find This Useful

Individuals interested in laboratory design, spectrometry, reaction kinetics, and regulatory compliance in chemical handling may find this discussion relevant.

androol
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I'm designing my lab and so I want a spectrometer to investigate reaction kinetics eh.

I am looking for a data logging spectrometer that can keep the reaction at constant temperature. My teacher is probably going to buy it. Does anyone know what company makes good spectrometers? About a couple thousand dollars maybe. I don't know my prof's budget, but the school's rich.
 
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What's your education level, and where are you going to build your lab? I would also be interested in hearing about some of the details of implementation. I'm not quite sure if it would be legal, however, be sure to adhere to the proper regulations of chemical disposal and the maintenance of chemicals, otherwise you may be facing a fine/jail time in the future.
 
NMR is a great way to do reaction kinetics if the rate of your reaction is compatable with the NMR time scale. Another good one is ReactIR, but that probably out of your price range (I think they are around $30,000), but I'm not positive of that. ReactIR is really only good if you have a nice IR peak to watch.
 
http://www.business.com/directory/industrial_goods_and_services/industrial_supplies/laboratory/analytical_instruments/spectrometers/

Ain't going to do your shopping for you --- you should get an idea of what's available for what kind of money if you snoop around on these listings.
 

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