Tube Furnace Fabrication: Any Tips or Recommendations?

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SUMMARY

The discussion focuses on the fabrication of a laboratory tube furnace capable of reaching temperatures equal to or exceeding 1300°C. Key components mentioned include Mullite tubes, Kanthal A-1 wire, Kaowool insulation, and ITC 100 HT ceramic paste. The user seeks recommendations for materials and components, specifically a thermocouple and thermometer, and discusses using a Variac for temperature control. The estimated budget for the project is approximately $500.

PREREQUISITES
  • Understanding of high-temperature materials, specifically Mullite and Kanthal A-1 wire.
  • Knowledge of thermal insulation techniques using Kaowool and ITC 100 HT ceramic paste.
  • Familiarity with thermocouples and temperature measurement devices.
  • Basic electrical engineering principles for designing circuits, including dimmer switches and Variac usage.
NEXT STEPS
  • Research advanced properties of Mullite and alternative high-temperature materials.
  • Learn about thermocouple types and their applications in high-temperature environments.
  • Explore circuit design for high-power applications, focusing on dimmer switches and Variac configurations.
  • Investigate the process of glassblowing for custom components like quartz glass test tubes.
USEFUL FOR

This discussion is beneficial for laboratory technicians, materials scientists, and hobbyists interested in high-temperature furnace fabrication and thermal management solutions.

KYPOWERLIFTER
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Hi All:

I plan on producing a laboratory tube furnace capable of = to or > 1300 C. Does anyone have any experience working with materials designed for these temps?

I have been pricing Mullite tubes: 500 mm L; ~34 ID; ~40mm OD, 18 G Kanthal A-1 wire (to be wrapped around the tube), Kaowool insulation blanket, and a piece of 'stove pipe' to be the outer tube.

Right now I have two questions:

1) Any suggestions as to the above components? By that I mean suggestions, as to better (in terms of quality and ability to take temperature), grades/types?

2) I need to purchase a thermocouple and thermometer. Recommendations? I also need to design a circuit to adjust power to the wire. What would you guys do and how would you arrange it? I was thinking some sort of dimmer switch (have to handle 2000W power @ 230V) parallel with a bulb as indicator?

Bear with me... When I get it going I'll make a how-to thread with pictures.

Thanks in advance
 
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Update:

I have located two Mullite tubes; one @ 83.00 and one @ 86.00

Kanthal A-1 Wire @ 15.00-20.00

ITC 100 HT ceramic paste @ 38.00

Kaowool 1" 2600F 2 ft2 @ 13.50

Variac (for temp control) ebay searching ~100.00

Stove pipe... 10.00-15.00

Thermocouple and thermometer with the TP 04 thermocouple 89.99 http://cgi.ebay.ca/ws/eBayISAPI.dll?ViewItem&item=260359668034&ssPageName=ADME:X:RTQ:CA:1123

Quartz glass test tube (with ground glass joint) for use inside furnace... ~100.00

I need to find a glassblower, I assume.

Suggestions/Thoughts? This is looking like a 500.00 project...
 
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