How to determine polyester epoxy content in drybend?

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In summary, to analyze the percentage weight of polyester epoxy content in a powder mixture, a good method would be to use FTIR with known standards of polyester and other ingredients to obtain spectra and use a Beer's law routine for quantification. However, it is important to consider potential interference from fillers, pigments, and additives such as UV stabilizers and antioxidants. Thin films of 1-3 microns should also be prepared using a 20 ton press with heated platens to reduce variation in film thickness.
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doolue
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I have a powder dry-bend mixed from polyester epoxy resin, fillers, pigment, other additives... I'm seeking for a method to analyze percentage weight of polyester epoxy content in this powder. So, could you prove an appropriate method to do it?

Thanks
 
  • #3
doolue said:
I have a powder dry-bend mixed from polyester epoxy resin, fillers, pigment, other additives... I'm seeking for a method to analyze percentage weight of polyester epoxy content in this powder. So, could you prove an appropriate method to do it?

Thanks

FTIR is a good technique, but fillers and pigments can interfere with IR analytical wavelengths. Organic pigments or inorganic pigments? What kind of UV stabilizers or antioxidants are present? Carbon black kills IR spectra. Titanium dioxide blocks out a good portion of the region. Most organic pigments will have functional groups similar to polyester. However, if the other ingredients don't interfere, make standards with known wt% of polyester. Obtain FTIR spectra and use a a good Beer's law routine for quant. Use the peak ratio method to reduce variation in film thickness (you have to make thin films 1 - 3 micron for analysis). You will need a 20 ton press with heated platens for the thin films.
 

Related to How to determine polyester epoxy content in drybend?

1. What is polyester epoxy content and why is it important to determine?

Polyester epoxy content refers to the percentage of polyester and epoxy resins present in a drybend material. It is important to determine because the ratio of these resins affects the properties and performance of the material, such as strength, durability, and chemical resistance.

2. What methods can be used to determine polyester epoxy content in drybend?

There are several methods for determining polyester epoxy content, including Fourier transform infrared (FTIR) spectroscopy, thermogravimetric analysis (TGA), and gas chromatography-mass spectrometry (GC-MS). Each method has its own advantages and limitations, and the most suitable method will depend on the specific properties of the drybend material.

3. Can the polyester epoxy content in drybend be determined by visual inspection?

No, the polyester epoxy content cannot be accurately determined by visual inspection alone. While the presence of certain physical characteristics, such as color and texture, can provide some indication of the resin content, it is necessary to use analytical methods for an accurate measurement.

4. How does the polyester epoxy content affect the properties of drybend?

The polyester epoxy content has a significant impact on the properties of drybend. A higher percentage of epoxy resin can result in a stronger and more rigid material, while a higher percentage of polyester resin can provide greater flexibility and impact resistance. The ratio of these resins can also affect chemical resistance and other performance characteristics.

5. Are there any standards or guidelines for determining polyester epoxy content in drybend?

Yes, there are several standard methods and guidelines available for determining polyester epoxy content in drybend. These include ASTM International standards such as ASTM D5224 for FTIR analysis and ASTM D2584 for TGA analysis. It is important to follow these standardized methods to ensure accurate and reliable results.

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