Your scintillator array needs to verify that a muon has entered the sensitive volume and has stopped. This usually requires at least 3 scintillators; Two scintillators, separated by ~10 cm or more of lead, copper, or other nonmagnetic high density material, in coincidence (10 nanoseconds or better) to determine the arrival of a minimum-ionizing particle. The coincidence circuit also needs a third scintillator in prompt anti-coincidence to verify that the stopping muon did indeed stop, and not exit the other side. All scintillator signals should be processed through a discriminator circuit so all minimum ionizing particles will produce a fixed amplitude output signal (NIM level (preferred) or a TTL signal). These three scintillators determine a "START" signal, which if possible is used to start a MCA (multichannel analyzer). The muon (probably a positive muon, more later) will decay with a positron with maximum energy of about 52 MeV. (See Michel rho parameter energy specrum in Fig. 1 in
http://arxiv.org/pdf/hep-ex/0311040v2
A fourth scintillator (maybe 10 by 10 by 20 cm) should be the sensitive volume in which the muon stops, and the mu-decay signal from this scintillator is used to generate a delayed STOP for the MCA. At first, the MCA oscillator should be set to advance the channel number count at ~50 nanoseconds per channel. So a 200-channel MCA would record about 10 microseconds (~5 lifetimes) of delay time.
Both positive and negative muons will stop in the stopping volume. Negative muons will form muonic atoms and likely form muonic (atomic) atoms and get captured by the nuclei in the stopping volume. These muons will give an anomalously short decay time (under 1 microsecond, if stopping volume material is over Z ~26).
The discriminator level on the stopping volume scintillator should be set to detect all electrons over ~ 10 MeV (See Fig. 1 above).
There will be a lot of background counts in all scintillators, especially the one used for the stopping volume. This whole setup will need to be well shielded with non-radioactive-contaminated high density material (lead or copper). Ideally, the background counting rate in the stopping volume scintillator is less that 1000 random singles counts per second (This is the most difficult shielding problem). This will assure that only ~1% of the STOP signals will be due to random background.
You need to be especially careful to properly set the discriminator thresholds properly. For a 10-cm thick stopping volume discriminator, it should be able to detect all non-stopping minimum ionizing muons (~ 20 MeV signal) when the prompt anti-coincidence signal is put into prompt coincidence with #s 1 and 2..
A simpler setup is to use the stopping-volume scintillator for both the MCA START and STOP signal. You will still need to set the discriminator sensitivity threshold with minimum ionizing particles (like cosmic rays).
What scintillators, phototubes, fast electronics, and MCA do you have?
Good luck. I hope this helps.
Bob S