Can my sample be contaminated by grease on a rotary evaporator?

  • Thread starter Thread starter Cyrus the great
  • Start date Start date
  • Tags Tags
    Evaporator Rotary
AI Thread Summary
Using grease on the ground glass joint of a rotary evaporator can potentially contaminate the sample if it comes into contact with the solvent. The grease may leach into the butanol during evaporation, affecting the purity of the sample. Proper cleaning and using grease sparingly can mitigate this risk. Ensuring that the joint is secure and that the grease does not enter the flask is crucial. Contamination from grease is a valid concern and should be addressed to maintain sample integrity.
Cyrus the great
Messages
23
Reaction score
0

Homework Statement



Before, I started to evaporate my solvent (butanol) by using rotary evaporator, I greased the ground glass joint holding my flask and bump trapper. Subsequently, I secured my flask sample and the trapper with Keck clip . Is there any possibility that my sample may have been contaminated by grease?

Homework Equations

The Attempt at a Solution

 
Physics news on Phys.org
Cyrus the great said:
using rotary evaporator
There's always something "following" you around --- you "adapt/learn to live with it."
 
Thread 'Confusion regarding a chemical kinetics problem'
TL;DR Summary: cannot find out error in solution proposed. [![question with rate laws][1]][1] Now the rate law for the reaction (i.e reaction rate) can be written as: $$ R= k[N_2O_5] $$ my main question is, WHAT is this reaction equal to? what I mean here is, whether $$k[N_2O_5]= -d[N_2O_5]/dt$$ or is it $$k[N_2O_5]= -1/2 \frac{d}{dt} [N_2O_5] $$ ? The latter seems to be more apt, as the reaction rate must be -1/2 (disappearance rate of N2O5), which adheres to the stoichiometry of the...
Back
Top