Experimental Set-up for EMISSION & REFLECTION Spectroscopy: Is it Easy?

AI Thread Summary
The discussion revolves around the challenges of setting up an experimental project for emission and reflection spectroscopy as part of a master's thesis. The participant expresses concern about their lack of experience and seeks guidance on whether this task is manageable. Respondents emphasize the importance of understanding the lab's research focus, prior experience with spectrophotometric measurements, and the specific systems to be studied. They suggest clarifying the expected signal strengths, accuracy requirements, and budget for the project. Additionally, there is a cautionary note about the importance of choosing the right mentor, as inadequate support could hinder progress in graduate research. The lab in question specializes in solid-state research, particularly Raman scattering, and possesses various equipment, although it is not well organized.
photon79
Messages
60
Reaction score
0
Hi,
I went to my proff to ask for my master thesis, he told me that you yourself have to do the experimental set-up for EMISSION AND REFLECTION SPECTROSCOPY ,,,but I am not that experienxed, anybody knows is it an easy task or...?
 
Chemistry news on Phys.org
photon79 said:
he told me that you yourself have to do the experimental set-up for EMISSION AND REFLECTION SPECTROSCOPY
This is all your prof said ??! :eek: Sadly, there's not enough information there for any of us to be able to help very much. Try and answer the following questions first :

1. What research happens at this lab ?
2. Does the lab have any history of spectrophotometric measurements in the past, and if so, what equipment does it possesses ?
3. What systems are expected to be studied ?
4. What are the expected signal strengths and what is the required level of accuracy ?
5. What is the allocated budget ?
 
photon79 said:
Hi,
I went to my proff to ask for my master thesis, he told me that you yourself have to do the experimental set-up for EMISSION AND REFLECTION SPECTROSCOPY ,,,but I am not that experienxed, anybody knows is it an easy task or...?

please don't take this the wrong way, but if you are asking an internet forum about how to go about your graduate research i think that you should strongly consider whether or not things are going to work out with this professor (or with yourself).

choose your mentor with care, or you may waste many years of your life.
 
1. What research happens at this lab ?
this is a solid state research institute
2. Does the lab have any history of spectrophotometric measurements in the past, and if so, what equipment does it possesses ?
they do raman scattering with solid samples probing for elementary excitations of electronic, lattice dynamical or magnetic origin
3. What systems are expected to be studied ?
this is new set-up they asked for, so i don't know what they are going to study, on solids (powder samples ) for sure.
4. What are the expected signal strengths and what is the required level of accuracy ?
no info.
5. What is the allocated budget ?
all needed tools are there, but scattered (laser sources, microscope,polarisers, electronic interface,etc) donno exactly the budget.
 
It seems like a simple enough question: what is the solubility of epsom salt in water at 20°C? A graph or table showing how it varies with temperature would be a bonus. But upon searching the internet I have been unable to determine this with confidence. Wikipedia gives the value of 113g/100ml. But other sources disagree and I can't find a definitive source for the information. I even asked chatgpt but it couldn't be sure either. I thought, naively, that this would be easy to look up without...
I was introduced to the Octet Rule recently and make me wonder, why does 8 valence electrons or a full p orbital always make an element inert? What is so special with a full p orbital? Like take Calcium for an example, its outer orbital is filled but its only the s orbital thats filled so its still reactive not so much as the Alkaline metals but still pretty reactive. Can someone explain it to me? Thanks!!
Back
Top