What is the Setup Called that Collects Water from the Cu Reduction Process?

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The discussion centers around a hydrogen generator setup, which includes various components like a flask, a drying tube, and a CuO sample. The reactions taking place involve zinc reacting with hydrochloric acid to produce hydrogen gas and zinc chloride, while the CuO sample undergoes reduction with hydrogen to yield copper and water. The drying tubes play a crucial role in capturing water vapor, with calcium chloride (CaCl2) used to absorb moisture, leading to a measurable change in mass that can be used for stoichiometric calculations. The setup is noted for its ability to track the loss of oxygen from CuO and the production of water, although it is not ideal for directly measuring hydrogen gas output. The second drying tube specifically collects water generated during the reduction of CuO. The discussion also touches on the hydration states of CaCl2, indicating that it can form various hydrates depending on the amount of water absorbed.
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What is this setup called?
 

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Hydrogen generator.
 
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I can't seem to find hydrogen generator on wikipedia or other chemistry sites. Could you direct me to a link or tell me how it works?
 
Actually this is more complicated, hydrogen generator is just a part of the setup, and I doubt this particular setup has any particular name.

Can you try to guess what are reactions taking place in the flask, in the tube with CuO sample and in the drying tubes?
 
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In the flask:
Zn + 2HCl -> ZnCl2 + H2

In the drying tube:
I am not sure - maybe something to do with the water vapour?

In the CuO sample:
H2 + CuO -> Cu + H2O
 
TT0 said:
In the drying tube:
I am not sure - maybe something to do with the water vapour?

Yes, water is captured by CaCl2 as hydration water. And (that's one of the most important things in this experiment) mass of CaCl2 changes. You can easily check by how much it changed, you can also easily check by how much mass of CuO changed during reduction. That gives a nice starting point for many stoichiometry experiments.
 
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I can't think of any equations for hydration of CaCl2, could you give me some hints? Or does it create one of these things: CaCl2.H2O?

That gives a nice starting point for many stoichiometry experiments.

So are you saying that this setup is good to calculate the amount of H2 and H2O? Also what does the second drying tube
 
TT0 said:
does it create one of these things: CaCl2.H2O?

Yes, there are several hydrates with different numbers of hydration waters, CaCl2⋅2H2O, CaCl2⋅2H4O and CaCl2⋅6H2O.

So are you saying that this setup is good to calculate the amount of H2 and H2O?

Hydrogen? No. But you can easily check how much oxygen was lost from the CuO and how much water was produced in this process.

Also what does the second drying tube

Its mass change during the experiment - why?
 
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Also what does the second drying tube
Its mass change during the experiment - why?

I didn't finished typing it seems. What I meant was what does the second drying tube do? Does it just collect water from the Cu reduction process?
 
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TT0 said:
Does it just collect water from the Cu reduction process?

Yes, that's exactly what it does.
 
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