Investigating effects on epoxy adhesive

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Discussion Overview

The discussion revolves around a scientific research project investigating the effects of various parameters on epoxy adhesive when cured using UV light. Participants explore factors such as adhesion, cohesive strength, and other properties, while considering different experimental conditions and measurements.

Discussion Character

  • Exploratory
  • Technical explanation
  • Experimental/applied

Main Points Raised

  • One participant suggests investigating the effects of UV light intensity and duration on properties like tensile strength, durometer hardness, shrinkage percentage, and adhesive strength.
  • Another participant proposes including the temperature during the cure phase and the duration and temperature of the post-cure phase as additional parameters.
  • A different participant raises the idea of considering humidity during the cure process or the presence of liquids as factors that might affect the adhesive properties.
  • One participant describes their limited lab equipment and outlines their experimental approach, which includes measuring linear shrinkage by injecting epoxy into a capillary tube and varying UV exposure duration to plot shrinkage over time.

Areas of Agreement / Disagreement

Participants present multiple competing views regarding additional parameters to investigate, and the discussion remains unresolved as to which factors are most critical to include in the research.

Contextual Notes

Limitations include the dependence on specific equipment available in the lab and the potential impact of unmeasured environmental factors such as humidity and liquid presence during curing.

Who May Find This Useful

Researchers and students interested in adhesive technology, materials science, and experimental design in the context of polymer chemistry may find this discussion relevant.

unscientific
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Hi, I am currently doing a scientific research regarding epoxy adhesive.

Basically, you shine UV light onto the adhesive, it hardens.

Im given certain parameters like, intensity of UV light and duration of exposure.

I am supposed to investigate effects of varying parameters on: adhesion, cohesive strength and other properties.

So far I did some research, the effects that I could investigate on are: Tensile at break(eg 8900 psi), Durameter hardness (eg D75), shrinkage percentage, % elongation at break and adhesive strength (eg 1000Pa).

I would like comments/suggestions on working on this project with these, or maybe add new parameters?

What I have in mind is plotting a graph of Intensity against adhesive strength under a fixed exposure time, while recording the tensile at break, durometer hardness etc.

Any improvements/suggestions?
 
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You might include temperature of the cure phase and the length of time and temperature of post cure phase.

Are you able to change the concentration of the cure agent?
 
How about humidity during cure, or maybe even the presence of liquids?
 
Ok, basically I am working in a lab that has limited equipment, several machines i found are the uv machine, which allows one to set the intensity, and duration (mins/hrs). There is also a durometer, (i haven't actually seen it) but my mentor tells me it does a "Sweeping" action at a force, while plotting a graph. I intend to maybe put cured adhesive (a droplet) onto a substrate and measure at which point willl the cured resin actually "break". Now I am currently working on the linear shrinkage, where I inject epoxy into a capillary tube and measure the length before the cure and after the cure. I think I will vary the duration of exposure to UV, and record plot a graph of %linear shrinkage over time of exposure.
What do you guys think? (3 more weeks till the end of the project)
 

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