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Preparation of Alkyl Halide from Alcohol

  1. Nov 9, 2006 #1
    Explain why the aqueous washing of your alkyl halide product from the reaction of t-butyl alcohol with concentrated HCL must be carried out quickly.

    Washing the product with aqueous NaOH would get rid of any traces of acid left by neutralizing it, but I don't understand what time has to do with the washings. Can anyone explain this to me?

  2. jcsd
  3. Nov 11, 2006 #2


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    Probably to reduce co-precipitation.
  4. Nov 15, 2006 #3
    water can act as an acid or a base. If water is left to stand with your t-butyl chloride you can eliminate a small amount, get back your t-butanol and lose some product.
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