Method for analyzing pure carbon

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To determine the presence of carbon in a sample, especially when it is suspected to be in a physical form rather than a chemical one, several analysis techniques can be employed. Spectrometry, including mass spectrometry, is recommended as a reliable method for identifying carbon. Additionally, burning the sample in pure oxygen and testing for carbon dioxide is a straightforward approach, though it is destructive. For non-destructive testing of carbon in crystalline forms such as nanotubes or graphene, using a spectrometer to analyze the spectrum of light or particle beams reflected or transmitted through the sample is effective. Proton beam analysis has also been mentioned as a method for identifying elements in unknown samples.
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I have a sample on which I think carbon is formed physically but not chemically. What is an analysis technique to determine that there is carbon for sure?
 
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Welcome to PF;
You have a black deposit on something?
You can analyse it with a spectrometer - or a mass-spectrograph.
Either is pretty sure.

You could burn it in pure oxygen and test for carbon-dioxide... (bubble though lime water)
 
Simon Bridge said:
Welcome to PF;
You have a black deposit on something?
You can analyse it with a spectrometer - or a mass-spectrograph.
Either is pretty sure.

You could burn it in pure oxygen and test for carbon-dioxide... (bubble though lime water)

what about a nondestructive test for carbon that's in a more crystalline form like nanotubes, graphene, etc? just curious, since in this case, you cannot burn it, mass spec it, or anything like that.
 
You use a spectrometer like I said: you shine something on the sample, like light or some sort of particle beam, and examine the spectrum of either the reflected or transmitted beam.

I have used 2 and 4MeV protons to determine the elements present in an unknown sample.
 
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